Reaktion #1369946

Reaktionsgleichung

carbamic acid chloride

1-phenylsulfonyl-1,3-diaza-cyclohexane-2-one

phosgene

→

1-Chlorocarbonyl-2-oxo-3-phenylsulfonyl-1,3-diaza-cyclohexane

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe product was recrystallized from acetone/petrolether

Vorschrift

This carbamic acid chloride was produced as described in Example 27 A from 6 parts by weight of 1-phenylsulfonyl-1,3-diaza-cyclohexane-2-one and 5 parts by weight of phosgene. The product was recrystallized from acetone/petrolether.

Quelle