Reaktion #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

Reaktionsgleichung

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
→
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

Edukte

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid

Reagenzien

Keine

Lösungsmittel

CO
methanol

Reaktionsbedingungen

Temperatur
100°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06444233B1uspto-grants-2002_09