Reaktion #1365271

Reaktionsgleichung

α-naphthoic acid hydrazide

hexachloroacetone

→

N-α-naphthoyl-N'-trichloroacetylhydrazine

Ausbeute 88.2%

Lösungsmittel

acetonitrile

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethus obtained
2. 2
   SonstigeThe precipitates formed
3. 3
   Filtrationwere recovered by filtration

Vorschrift

To a mixture of 100 ml of acetonitrile and 14.6 g (0.055 mol) of hexachloroacetone was added 9.3 g of α-naphthoic acid hydrazide thus obtained and the resultant mixture was refluxed with stirring for 4 hours. The precipitates formed were recovered by filtration to provide 14.6 g (yield 88%) of N-α-naphthoyl-N'-trichloroacetylhydrazine.

Quelle