Reaktion #1344691

Reaktionsgleichung

didodecyl ether

isododecanol

trifluoromethanesulfonic acid

isododecene

→

Isododecane

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturheated for 1.5 h to 240° C
2. 2
   SonstigeThe organic phase of the distillate obtained (171.9 g)
3. 3
   Trocknenwas dried over sodium sulfate
4. 4
   Sonstigethe product was isolated by filtration)

Vorschrift

300.0 g Lial® 123 (isododecanol from Sasol) and 18.0 g trifluoromethanesulfonic acid (50% by weight in water) were introduced into a distillation apparatus and heated for 1.5 h to 240° C. The organic phase of the distillate obtained (171.9 g) was dried over sodium sulfate and the product was isolated by filtration). The product then contained 91.5% isododecene, 7.5% Lial® 123 and 1.0% didodecyl ether (GC analysis).

Quelle