Reaktion #1332434

Reaktionsgleichung

di-p-tolylamine

potassium carbonate

dibromobenzo[a]perylene

→

bis(di-p-tolylamino)benzo[a]perylene

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis mixture stood still for reaction at 200 degrees centigrade for thirty hours
2. 2
   Extraktionwas extracted by chloroform

Vorschrift

Then, two equivalents of di-p-tolylamine, potassium carbonate, and copper power were added to the thus obtained dibromobenzo[a]perylene. This mixture stood still for reaction at 200 degrees centigrade for thirty hours. After reactant solution was diluted with water, reactant was extracted by chloroform. Thereafter, the reactant was refined in a conventional manner to thereby obtain bis(di-p-tolylamino)benzo[a]perylene.

Quelle