Reaktion #1266960

ord-7c7e4de39abb45afacbe6d47a945bbca

Reaktionsgleichung

Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(O)ccc12
3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
C[n+]1ccn(C(=O)N2CCOCC2)c1.[I-]
3-(morpholine-4-carbonyl)-1-methyl-3H-imidazol-1-ium iodide
→
Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(OC(=O)N3CCOCC3)ccc12
title compound
Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(OC(=O)N3CCOCC3)ccc12
Morpholine-4-carboxylic acid 3-(3,4-dichloro-benzyl)-4-methyl-2-oxo-2H-chromen-7-yl ester

Edukte

Cc1c(Cc2ccc(Cl)c(Cl)c2)c(=O)oc2cc(O)ccc12
3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one
C[n+]1ccn(C(=O)N2CCOCC2)c1.[I-]
3-(morpholine-4-carbonyl)-1-methyl-3H-imidazol-1-ium iodide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 3-(3,4-dichloro-benzyl)-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(morpholine-4-carbonyl)-1-methyl-3H-imidazol-1-ium iodide. HPLC-MS m/z=448 (M+1), Rt: 4.73 min.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07279470B2uspto-grants-2007_10