Reaktion #1256724

ord-8ab2b15329334edda2b86425c20bd320

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    FiltrationThe solution is filtered
  2. 2
    Sonstigeevaporated

Vorschrift

8.60 g (30 mmol) of 3-ethoxy-8-propyl-7,8,9,10-tetrahydrobenzo[c]-chromen-6-one are dissolved in THF and hydrogenated to cessation on palladium/active carbon. The solution is filtered and evaporated, giving 3-ethoxy-8-propyl-6a,7,8,9,10,10a-hexahydrobenzo[c]chromen-6-one as colourless oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07824745B2uspto-grants-2010_11