Reaktion #1245600

Reaktionsgleichung

N-(2-hydroxy-1,1-dimethyl-ethyl)-acetamide

piperidin-4-yl-methanol

CH3CN H2O

CH3CN H2O

CH3CN

→

title compound

1-(4-Hydroxymethyl-piperidin-1-yl)-ethanone

Lösungsmittel

H2O

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstige0.39 min.

Vorschrift

The title compound is prepared analogously as described for N-(2-hydroxy-1,1-dimethyl-ethyl)-acetamide from piperidin-4-yl-methanol. MS (LC-MS): [M+H]+=158.3. tR (HPLC, Waters Symmetry C18 column, 5-95% CH3CN/H2O/3.5 min, 95% CH3CN/H2O, 2 min, CH3CN and H2O containing 0.1% TFA, flow: 0.6 mL/min): 0.39 min.

Quelle