Reaktion #1193846

Reaktionsgleichung

Hydrochloric acid ethyl acetate

N-[3-(dimethylamino)propyl]-[2-(1-octadecanoyl-2-piperidyl)ethoxy]formamide

→

compound

N-[3-(Dimethylamino)propyl]-[2-(1-octadecanoyl-2-piperidyl)ethoxy]formamide hydrochloride

Lösungsmittel

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenthe reaction mixture was concentrated
2. 2
   SonstigeThe residue was recrystallized with ethyl acetate

Vorschrift

4N Hydrochloric acid/ethyl acetate solution (0.20 ml) was added to a solution of N-[3-(dimethylamino)propyl]-[2-(1-octadecanoyl-2-piperidyl)ethoxy]formamide (0.200 g) in ethyl acetate (2 ml). After being stirred for 15 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.183 g) as white crystals.

Quelle