Reaktion #1178194

ord-ebbd8bfece5b4b7a8c778409133d6494

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Filtrationfiltered
  2. 2
    SonstigeThe methanol is evaporated

Vorschrift

3.5 g of 2-nitro-3-hydroxy-6-methylpyridine in 50 ml of methanol are placed under hydrogen pressure in the presence of one gram of palladinized charcoal. The mixture is stirred and filtered. The methanol is evaporated.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05084456uspto-grants-1992_01