Reaktion #11757

Reaktionsgleichung

5-chloro-2-methoxybenzene sulfonyl chloride

ammonia

→

title compound

5-Chloro-2-methoxy-benzenesulfonamide

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe white solid that precipitated out of solution
2. 2
   Filtrationwas collected by filtration
3. 3
   Waschenwashed with dichloromethane

Vorschrift

To a solution of 5-chloro-2-methoxybenzene sulfonyl chloride (1.0 g, 4.15 mmol) in tetrahydrofuran (10 mL) was bubbled ammonia gas until saturated. The reaction was stirred overnight. The white solid that precipitated out of solution was collected by filtration and washed with dichloromethane to give the title compound (0.52 g).

Quelle