Reaktion #1165574

ord-d1a7d4c714c94a28b646e1624ebf0e25

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

In a similar manner to Example 52d, a solution of N-[1-(4-chlorophenyl)-1-methylethyl]-8-(imidazol-1-yl)octanamide (5.9 g) in THF (130 ml) was reduced with BH3/THF (64.5 ml of a 1M solution) to give N-[1-(4-chlorophenyl)-1-methylethyl]-8-(imidazol-1-yl)octylamine, b.p. 210° C. (0.05 mmHg).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05547972uspto-grants-1996_08