Reaktion #1163392

Reaktionsgleichung

3-methoxy-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepine-11-thione

amino acetaldehyde dimethyl acetal

→

[(5H-dibenzo[b,e][1,4]diazepin-11-yl)amino]acetaldehyde dimethyl acetal

Lösungsmittel

n-butanol

Reaktionsbedingungen

Vorschrift

In the manner given in Example 4, 3-methoxy-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepine-11-thione is treated with amino acetaldehyde dimethyl acetal in n-butanol to give [(5H-dibenzo[b,e][1,4]diazepin-11-yl)amino]acetaldehyde dimethyl acetal.

Quelle