Reaktion #1161419

ord-74d84d546d114887a92222d2404c8457

Reaktionsgleichung

COC(=O)C(Br)CCBr
methyl-2,4-dibromobutyrate
CN
methylamine
CNC(=O)C(Br)CCBr
N-methyl-2,4-dibromobutyramide

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeIn a second step of the reaction

Vorschrift

In a second step of the reaction, the methyl-2,4-dibromobutyrate is reacted with methylamine in an aqueous solution at a temperature of below ambient in order to form N-methyl-2,4-dibromobutyramide. Then butyramide is then recovered and purified to obtain the solid intermediate product.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04973708uspto-grants-1990_11