Reaktion #1161377

ord-2f200fbf9ca442f48ee8412b072d1953

Reaktionsgleichung

Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
product
Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
2-[(4-Chloro-2-nitrophenyl)thio]-1-methyl-1H-imidazole
Cl
hydrogen chloride
→
Cl.Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
product
Cl.Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
2-[(4-Chloro-2-nitrophenyl)thio]-1-methyl-1H-imidazole hydrochloride

Edukte

Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
product
Cn1ccnc1Sc1ccc(Cl)cc1[N+](=O)[O-]
2-[(4-Chloro-2-nitrophenyl)thio]-1-methyl-1H-imidazole
Cl
hydrogen chloride

Reagenzien

Keine

Lösungsmittel

ClCCl
dichloromethane
CCOCC
ether

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The product from Example 19 was treated with hydrogen chloride in dichloromethane and ether to give the product as yellow prisms mp 155°-160° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04973599uspto-grants-1990_11