Reaktion #1160666

Reaktionsgleichung

sodium acetate

vinyl acetate

lauric acid

→

vinyl laurate

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISSOLUTIONThe acid was dissolved
2. 2
   Temperaturby warming
3. 3
   Temperaturthe reaction mixture was heated
4. 4
   Temperaturunder reflux for 3 hours
5. 5
   Temperaturto cool to ambient temperature

Vorschrift

51.5 g of vinyl acetate and 20 g (0.1 mole) of lauric acid were introduced into a 100-ml two-necked round-bottomed flask. The acid was dissolved by warming and 0.4 g of mercuric acetate was added under a stream of nitrogen. The mixture was thus maintained for 30 minutes at ambient temperature, with magnetic stirring, under nitrogen. Two drops of sulfuric acid (95%) were then added and the reaction mixture was heated under reflux for 3 hours. It was then permitted to cool to ambient temperature and 0.21 g of sodium acetate was then added.

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