Reaktion #1154663

ord-cfd6f93fa97547bf9f1b3d8da32ec84f

Reaktionsgleichung

Cc1nc(-c2ccc(N)cc2)no1
4-(5-methyl-1,2,4-oxadiazol-3-yl)-aniline
CCOC(=O)CBr
ethyl bromoacetate
→
CCOC(=O)CNc1ccc(-c2noc(C)n2)cc1
Ethyl 4-(5-methyl-1,2,4-oxadiazol-3-yl)-phenylamino-acetate

Edukte

Cc1nc(-c2ccc(N)cc2)no1
4-(5-methyl-1,2,4-oxadiazol-3-yl)-aniline
CCOC(=O)CBr
ethyl bromoacetate

Reagenzien

Keine

Lösungsmittel

CCN(C(C)C)C(C)C
N-ethyl-diisopropylamine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared analogously to Example 9a from 4-(5-methyl-1,2,4-oxadiazol-3-yl)-aniline and ethyl bromoacetate in N-ethyl-diisopropylamine.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06248770B1uspto-grants-2001_06