Reaktion #1153330

ord-206581dde5bb4a38ab11d43fe4ac163c

Reaktionsgleichung

O=[N+]([O-])c1ccc2c(c1)S(=O)(=O)N=C(n1ccnc1)N2.c1c[nH+]c[nH]1
3-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt
NC1CCC1
cyclobutylamine
→
O=[N+]([O-])c1ccc2c(c1)S(=O)(=O)N=C(NC1CCC1)N2
title compound
O=[N+]([O-])c1ccc2c(c1)S(=O)(=O)N=C(NC1CCC1)N2
3-Cyclobutylamino-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide

Edukte

O=[N+]([O-])c1ccc2c(c1)S(=O)(=O)N=C(n1ccnc1)N2.c1c[nH+]c[nH]1
3-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt
NC1CCC1
cyclobutylamine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

3-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt was treated with cyclobutylamine according to the general procedure Method D to give the title compound; m.p. 298-301° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06242443B1uspto-grants-2001_06