Reaktion #1152922

ord-cba2002bf722486e97dfbc4f4ed88723

Reaktionsgleichung

C=C(C(=O)OC)c1ccccc1
methyl atropate
CCCCCCCC/C=C\CCCCCCCC(=O)O
oleic acid
COC(=O)C(=O)c1ccccc1
methyl benzoylformate
Ausbeute 88.0%

Reagenzien

Keine

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe co-oxidation reaction

Vorschrift

The co-oxidation reaction was carried out in manner as described in Example 16, except that methyl atropate was used in lieu of oleic acid. As a result, acetic acid was obtained at a yield of 95% and methyl benzoylformate was obtained at a yield of 88%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04331608uspto-grants-1982_05