Reaktion #1147873

ord-8d622ae6515e4225b45688c55e5e62c4

Reaktionsgleichung

CN(C)c1ccc(N=Nc2ccc(S(=O)(=O)Cl)cc2)cc1
4-dimethylaminoazobenzene-4′-sulfonyl chloride
CCOCc1nc2c(N)nc(C)c(C)c2n1CCC1CCNCC1
2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine
CCOCc1nc2c(N)nc(C)c(C)c2n1CCC1CCN(S(=O)(=O)c2ccc(N=Nc3ccc(N(C)C)cc3)cc2)CC1
desired product
CCOCc1nc2c(N)nc(C)c(C)c2n1CCC1CCN(S(=O)(=O)c2ccc(N=Nc3ccc(N(C)C)cc3)cc2)CC1
1-(2-{1-[4-(4-Dimethylaminophenylazo)benzenesulfonyl]piperidin-4-yl}ethyl)-2-(ethoxymethyl)-6,7-dimethyl-1H-imidazo[4,5-c]pyridin-4-amine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using the method of Examples 49-56, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired product. The observed accurate mass was 619.3185.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06525064B1uspto-grants-2003_02