Reaktion #1146219

ord-379597fab6b9495dad5b9a0e2fffc288

Reaktionsgleichung

C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
compound ( 204 )
C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
CC(C)(C)NC(=O)C(C)(C)N(O)C(C)(C)C
tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine
C=C(C)CCl
methallylchloride
→
C=C(C)CON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-methallyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
Ausbeute 84.0%

Edukte

C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
compound ( 204 )
C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
CC(C)(C)NC(=O)C(C)(C)N(O)C(C)(C)C
tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine
C=C(C)CCl
methallylchloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The compound is prepared in analogy to compound (204) from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and methallylchloride in 84% yield as colorless oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06518326B1uspto-grants-2003_02