Reaktion #1146218

ord-9d28527cf9954cc2b5c278a97c1acd60

Reaktionsgleichung

C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
compound 204
C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
CC(C)(C)NC(=O)C(C)(C)N(O)C(C)(C)C
tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine
C=CC=CCBr
1-brom-2,4-pentadien
→
C=CC=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-(2.4-pentadienyloxy)-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
Ausbeute 80.0%

Edukte

C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
compound 204
C=CCON(C(C)(C)C)C(C)(C)C(=O)NC(C)(C)C
N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
CC(C)(C)NC(=O)C(C)(C)N(O)C(C)(C)C
tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine
C=CC=CCBr
1-brom-2,4-pentadien

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The compound is prepared in analogy to compound 204 from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and 1-brom-2,4-pentadien in 80% yield as colorless oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06518326B1uspto-grants-2003_02