Reaktion #1144997
ord-70b5fe82cc19412f8a4f5ec0e7788ea6
Reaktionsgleichung
Reagenzien
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1FiltrationThe reaction mixture was filtered through a short pad of silica gel
- 2Einengenconcentrated in vacuo
Vorschrift
A solution of 4-(4-fluorophenoxy)-2-allylphenol (2.30 g, 9.42 mmol) and 5% Pd/C (0.90 g) in ethyl acetate (30 mL) was stirred under H2 atmosphere for 3 h at room temperature. The reaction mixture was filtered through a short pad of silica gel and concentrated in vacuo to afford the title compound which was used as is.