Reaktion #1144997

ord-70b5fe82cc19412f8a4f5ec0e7788ea6

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    FiltrationThe reaction mixture was filtered through a short pad of silica gel
  2. 2
    Einengenconcentrated in vacuo

Vorschrift

A solution of 4-(4-fluorophenoxy)-2-allylphenol (2.30 g, 9.42 mmol) and 5% Pd/C (0.90 g) in ethyl acetate (30 mL) was stirred under H2 atmosphere for 3 h at room temperature. The reaction mixture was filtered through a short pad of silica gel and concentrated in vacuo to afford the title compound which was used as is.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06515015B1uspto-grants-2003_02