Reaktion #1135817

Reaktionsgleichung

3-trifluoromethyl-2-methylbenzoic acid

oxalyl dichloride

N,N-dimethylformamide

→

3-trifluoromethyl-2-methylbenzoic acid chloride

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe reaction mixtures
2. 2
   Einengenwere concentrated under reduced pressure

Vorschrift

A mixture of 3-trifluoromethyl-2-methylbenzoic acid 5.00 g, oxalyl dichloride 3.42 g, N,N-dimethylformamide about 50 mg and tetrahydrofuran 200 mL was stirred at 25° C. for one hour. The reaction mixtures were concentrated under reduced pressure to give 3-trifluoromethyl-2-methylbenzoic acid chloride.

Quelle