Reaktion #1135813

Reaktionsgleichung

1-ethoxy-2-methyl-3-nitrobenzene

→

3-ethoxy-2-methylaniline

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe mixtures were filtered
2. 2
   Einengenthe filtrates were concentrated

Vorschrift

A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.

Quelle