Reaktion #1134642

Reaktionsgleichung

compound

2-amino-9-(4-hydroxy-3-hydroxymethyl-2-methylene-cyclopentyl)-1,9-dihydropurin-6-one

N,N-dimethylformamide

→

title compound

Ausbeute 85.6%

2-amino-9-(4-hydroxy-3-hydroxymethyl-2-methylene-cyclopentyl)-1,9-dihydro-purin-6-one N,N-dimethylformamide

Ausbeute 85.6%

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe resulting solution was filtered

Vorschrift

The compound obtained in Example 1-9 (1 g) was added to N,N-dimethylformamide (5 ml) and stirred at room temperature for 2 hrs and at 0° C. for 1 hr. The resulting solution was filtered to obtain the title compound as a white-colored solid (0.95 g, yield: 85.6%).

Quelle