Reaktion #1121771

Reaktionsgleichung

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas heated
2. 2
   Temperaturat reflux for 90 mins
3. 3
   EinengenThe reaction mixture was concentrated under reduced pressure
4. 4
   Sonstigeto give an oil
5. 5
   Sonstigeyield 5.77 parts of the following structure

Vorschrift

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

Quelle