Reaktion #1118714

ord-aaf35d178a044ec78e1b48b0f91d8554

Reaktionsgleichung

Cn1nc(C2CCCCC2)cc1N
3-cyclohexyl-1-methyl-5-pyrazolamine
COC(=O)C(=Cc1cccc([N+](=O)[O-])c1)C(C)=O
methyl-2-(3-nitrobenzyliden)acetoacetate
→
COC(=O)C1=C(C)Nc2c(c(C3CCCCC3)nn2C)C1c1cccc([N+](=O)[O-])c1
3-Cyclohexyl-4,7-dihydro-1,6-dimethyl-4-(3-nitrophenyl)-1H-pyrazolo[3,4-b]pyridin-5-carboxylic acid methyl ester

Edukte

Cn1nc(C2CCCCC2)cc1N
3-cyclohexyl-1-methyl-5-pyrazolamine
COC(=O)C(=Cc1cccc([N+](=O)[O-])c1)C(C)=O
methyl-2-(3-nitrobenzyliden)acetoacetate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Starting from 3-cyclohexyl-1-methyl-5-pyrazolamine and methyl-2-(3-nitrobenzyliden)acetoacetate in equimolar proportions.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04954508uspto-grants-1990_09