Reaktion #1108148
ord-99f5706563e94938a082bb3edd44fd6d
Reaktionsgleichung
coumarin
heptadecanoic acid
→
heptadecanal
Ausbeute 21.0%
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeAfter the reaction
- 2Temperaturthe autoclave was cooled with ice
- 3Sonstigewas obtained in a yield of 78%
Vorschrift
After the reaction, the autoclave was cooled with ice, and the pressure was reduced; subsequently, the reaction mixture was analyzed by FT-NMR using coumarin as an internal standard. The results confirmed that heptadecanoic acid was obtained in a yield of 78%, and heptadecanal was obtained in a yield of 21%.