Reaktion #1108148

ord-99f5706563e94938a082bb3edd44fd6d

Reaktionsgleichung

O=c1ccc2ccccc2o1
coumarin
CCCCCCCCCCCCCCCCC(=O)O
heptadecanoic acid
CCCCCCCCCCCCCCCCC=O
heptadecanal
Ausbeute 21.0%

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAfter the reaction
  2. 2
    Temperaturthe autoclave was cooled with ice
  3. 3
    Sonstigewas obtained in a yield of 78%

Vorschrift

After the reaction, the autoclave was cooled with ice, and the pressure was reduced; subsequently, the reaction mixture was analyzed by FT-NMR using coumarin as an internal standard. The results confirmed that heptadecanoic acid was obtained in a yield of 78%, and heptadecanal was obtained in a yield of 21%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08716501B2uspto-grants-2014_05