Reaktion #1106669

ord-f5ff3aa120644be0be915121f0436399

Reaktionsgleichung

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin
→
COCCNc1cccc2c1C(=O)c1cccc(NCCN(C)C)c1C2=O
2-(dimethylamino) ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

Edukte

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis product was used in the next step without any purification

Vorschrift

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08715944B2uspto-grants-2014_05