Reaktion #1106665

Reaktionsgleichung

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwas refluxed for 18 h
2. 2
   Sonstigeto precipitate the title compound which
3. 3
   Sonstigewas recrystallised from methanol

Vorschrift

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

Quelle