Reaktion #1106645

ord-5deaa066f335434bad96507e8dfca8df

Reaktionsgleichung

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1cn[nH]c1
pyrazole LiTFSI
Ausbeute 137.4%

Edukte

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
30°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

2.13 g of purified pyrazole and 3 g of LiTFSI were put into a round bottom flask and slowly stirred for 5 hours under a nitrogen circumstance of 30° C., thereby obtaining 5.1 g of pyrazole-LiTFSI eutectic mixture.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08715866B2uspto-grants-2014_05