Reaktion #1106643

ord-c7c21d9897bb41fca3c57edbb966395d

Reaktionsgleichung

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1c[nH]cn1
imidazole LiTFSI
Ausbeute 137.4%

Edukte

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
40°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

14.2 g of purified imidazole and 20 g of LiTFSI were put into a round bottom flask and slowly stirred for 2 hours under a nitrogen circumstance of 40° C., thereby obtaining 34 g of imidazole-LiTFSI eutectic mixture.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08715866B2uspto-grants-2014_05