Reaktion #11037

ord-c673a36413bb4095a3c1e179447fff08

Reaktionsgleichung

CC(C)(C)c1ccc2c(c1)Cc1cc(C(C)(C)C)cc(Br)c1-2
4-bromo-2,7-di-t-butyl-fluorene
[Al+3].[Cl-].[Cl-].[Cl-]
AlCl3
→
Brc1cccc2c1-c1ccccc1C2
4-bromo-fluorene

Edukte

CC(C)(C)c1ccc2c(c1)Cc1cc(C(C)(C)C)cc(Br)c1-2
4-bromo-2,7-di-t-butyl-fluorene
[Al+3].[Cl-].[Cl-].[Cl-]
AlCl3

Reagenzien

Keine

Lösungsmittel

c1ccccc1
benzene

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The 4-bromo-2,7-di-t-butyl-fluorene is then reacted with benzene and AlCl3 to produce 4-bromo-fluorene as follows:

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07094938B1uspto-grants-2006_08