Reaktion #1094396

ord-dc6e6bd013354151bf0ee6c3a0bab6c2

Reaktionsgleichung

O=C(Cl)c1ccc(Cl)nc1
6-chloronicotinic chloride
CC(C)(C)c1ccc(N)c([N+](=O)[O-])c1
4-(t-butyl)-2-nitroaniline
CC(C)(C)c1ccc(NC(=O)c2ccc(Cl)nc2)c([N+](=O)[O-])c1
title compound
CC(C)(C)c1ccc(NC(=O)c2ccc(Cl)nc2)c([N+](=O)[O-])c1
6-Chloro-N-(4-t-butyl-2-nitrophenyl)-3-pyridinecarboxamide

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 6-chloronicotinic chloride and 4-(t-butyl)-2-nitroaniline as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.30 (s, 1H), 9.03 (d, J=2.1, 1H), 8.83 (d, J=9.0, 1H), 8.29 (d, J=2.7, 1H), 8.25-8.21 (m, 1H), 7.80-7.76 (m, 1H), 7.52 (d, J=8.4, 1H), 1.38 (s, 9H).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06794397B2uspto-grants-2004_09