Reaktion #10915

ord-00c077eb05ac42d3b480fa4c391efc38

Reaktionsgleichung

N#CN
cyanamide
S=C=Nc1ccc(N2CCN(CC3CC3)CC2)cc1
1-(4-isothiocyanatophenyl)-4-cyclopropylmethylpiperazine
S=C=Nc1ccc(N2CCN(CC3CC3)CC2)cc1
1-(4-Isothiocyanatophenyl)-4-(1-cyclopropylmethyl)piperazine
O=C(CBr)c1ccc(O)c(F)c1
2-bromo-1-(3-fluoro-4-hydroxyphenyl)ethanone
Nc1nc(Nc2ccc(N3CCN(CC4CC4)CC3)cc2)sc1C(=O)c1ccc(O)c(F)c1
{4-Amino-2-[4-(4-cyclopropylmethyl-piperazin-1-yl)-phenylamino]-thiazol-5-yl}-(3-fluoro-4-hydroxy-phenyl)-methanone

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

This compound was prepared from cyanamide, 1-(4-isothiocyanatophenyl)-4-cyclopropylmethylpiperazine (of Example 14G) and 2-bromo-1-(3-fluoro-4-hydroxyphenyl)ethanone (of Example 14M) following the procedure used in Example 24. Mass spectrum (ES) MH+=468.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07094896B2uspto-grants-2006_08