Reaktion #1078344

Reaktionsgleichung

1,2,4-triazole

tris(pentafluorophenyl)borane

dioctadecylmethylamine

→

Dioctadecylmethylammonium bis(tris(Pentafluorophenyl)borane) 1,2,4-triazolide

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturrefluxed under argon for 5 hours
2. 2
   SonstigeYield

Vorschrift

1,2,4-triazole (0.1349 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for 5 hours. The volatiles were then stripped under vacuum. Yield, 2.702 g, 84.92 percent.

Quelle