Reaktion #1078342

Reaktionsgleichung

4,5-dichloroimidazole

tris(pentafluorophenyl)borane

dioctadecylmethylamine

→

Dioctadecylmethylammonium bis(tris(Pentafluorophenyl)borane) 4,5-dichloroimidazolide

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturrefluxed under argon for hours
2. 2
   SonstigeYield

Vorschrift

4,5-dichloroimidazole (0.2675 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for hours. The volatiles were then stripped under vacuum. Yield, 2.937 g, 88.62 percent.

Quelle