Reaktion #1078341

Reaktionsgleichung

5,6-dimethylbenzimidazole

tris(pentafluorophenyl)borane

dioctadecylmethylamine

→

Dioctadecylmethylammonium bis(tris(Pentafluorophenyl)borane) 5,6-dimethylbenzimidazolide

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturrefluxed under argon for 16 hours
2. 2
   SonstigeYield

Vorschrift

5,6-dimethylbenzimidazole (0.2855 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for 16 hours. The volatiles were then stripped under vacuum. Yield, 3.060 g, 91.84 percent.

Quelle