Reaktion #1076186

ord-37a8b151357044feb540d0a6fe07f897

Reaktionsgleichung

Nc1cnccn1
2-aminopyrazine
[C-]#[N+]C(C)(C)C
tert-butyl isocyanide
O=Cc1c2ccccc2cc2ccccc12
anthracene-9-carbaldehyde
→
CC(C)(C)Nc1c(-c2c3ccccc3cc3ccccc23)nc2cnccn12
Compound ( 30 )
CC(C)(C)Nc1c(-c2c3ccccc3cc3ccccc23)nc2cnccn12
(2-Anthracen-9-yl-imidazo[1,2-a]pyrazin-3-yl)-tert-butyl-amine

Edukte

Nc1cnccn1
2-aminopyrazine
[C-]#[N+]C(C)(C)C
tert-butyl isocyanide
O=Cc1c2ccccc2cc2ccccc12
anthracene-9-carbaldehyde

Reagenzien

Keine

Lösungsmittel

[O-][Cl+3]([O-])([O-])O
perchloric acid

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Compound (30) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyrazine solution (0.1 M, MC), 0.575 ml tert-butyl isocyanide solution (0.2 M, MC), 0.500 ml anthracene-9-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 366.5; found mass 367.3 (ESI-MS)

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06638933B2uspto-grants-2003_10