Reaktion #1073160

ord-9294e126bd8b47b9b7be998f2dfcd389

Reaktionsgleichung

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCCCCCCCCCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Dodecyl-N-(2-amino-2-deoxy-glucopyranosyl)-amine hydrochloride

Edukte

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONwere added
  2. 2
    Sonstigethe product precipitated
  3. 3
    ExtraktionThe solid was extracted three times
  4. 4
    workup.STIRRINGby stirring with ether
  5. 5
    Filtrationfiltered off with suction
  6. 6
    Sonstigedried under a high vacuum

Vorschrift

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04710491uspto-grants-1987_12