Reaktion #1073158

ord-f10767dfc78d4c6c802fb1156d989e2b

Reaktionsgleichung

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Propyl-(2-amino-2-deoxy-D-glucopyranosyl)-amine hydrochloride

Edukte

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

Reagenzien

Keine

Lösungsmittel

CCCN
n-propylamine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturthe suspension was warmed to 70°, until a clear solution
  2. 2
    Sonstigewas formed
  3. 3
    Sonstigethe product precipitated

Vorschrift

21.5 g of glucosamine hydrochloride were suspended in 17.7 g of n-propylamine and the suspension was warmed to 70°, until a clear solution was formed. On cooling to room temperature, the product precipitated.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04710491uspto-grants-1987_12