Reaktion #1058658

ord-8c4b3263c4b04675b6eb1f480e12df65

Reaktionsgleichung

Cn1ccnc1
1-methylimidazole
CC(=S)OCCl
chloromethylthioacetate
→
CC(=S)OC[n+]1ccn(C)c1.[Cl-]
1-THIOACETYLOXYMETHYL-3-METHYLIMIDAZOLIUM CHLORIDE

Edukte

Cn1ccnc1
1-methylimidazole
CC(=S)OCCl
chloromethylthioacetate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturwith cooling
  2. 2
    workup.WAITwas left
  3. 3
    workup.WAITstoppered at room temperature overnight

Vorschrift

To 0.7 g (8.52 millimoles) of 1-methylimidazole was added slowly and with cooling, 1.5 g of (16.2 millimoles) chloromethylthioacetate. The solution solidified in 10 minutes and was left stoppered at room temperature overnight.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04160099uspto-grants-1979_07