Reaktion #1057984

Reaktionsgleichung

4-Chloromethylbenzoic acid

borane THF

→

4-chloromethylbenzyl alcohol

Ausbeute 79.8%

4-Chloromethylbenzyl alcohol

Ausbeute 79.8%

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigequenched with excess methanol
2. 2
   SonstigeEvaporation

Vorschrift

4-Chloromethylbenzoic acid (20 mmol) was dissolved in 20 ml THF, then 30 ml borane/THF were added. The mixture was stirred for 16 hrs at room temperature, and then quenched with excess methanol. Evaporation yielded about 2.5 g 4-chloromethylbenzyl alcohol 36.

Quelle