Reaktion #1055022

ord-79188916946d46fe8b9061c115a7a70d

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared according to the procedure described in step 2 of Example 18 from phenyl 2-{4-[2-ethyl-4-(2-pyridinyl)-1H-imidazol-1-yl]phenyl}ethylcarbamate and 4-chlorobenzenesulfonamide. MS (ESI) m/z 510 [M+H]+, 508 [M−H]−, 1H-NMR (CDCl3) □1.17 (3H, t, J=7.3 Hz), 2.65 (2H, q, J=7.7 Hz), 2.80-2.88 (2H, m), 3.42-3.55 (2H, m), 6.78 (1H, br), 7.15-7.28 (4H, m),7.42 (2H, d, J=8.4 Hz), 7.58 (1H, s), 7.71 (1H, t, J=6.0 Hz), 7.80-7.89 (3H, m), 8.51 (1H, d, J=6.0 Hz).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06956050B2uspto-grants-2005_10