Reaktion #1055019

ord-e25a5811901f428992744298d6ac8144

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared according to the procedure described in step 2 of Example 18 from phenyl 2-{4-[2-ethyl-4-(4-fluorophenyl)-1H-imidazol-1-yl]phenyl}ethylcarbamate and 4-chlorobenzenesulfonamide. MS (ESI) m/z 527 [M+H]+, 525 [M−H]−, 1H-NMR (CDCl3) δ 1.24 (3H, t, J=7.5 Hz), 2.69 (2H, q, J=7.5 Hz), 2.83-2.90 (2H, m), 3.45-3.54 (2H, m), 6.50 (1H, br), 7.05 (2H, t, J=8.8 Hz), 7.18 (1H, s), 7.22-7.30 (2H, m), 7.42-7.52 (3H, m), 7.70-7.79 (4H, m).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06956050B2uspto-grants-2005_10