Reaktion #1054534
ord-982b82a241964626b2262cc05b40d0c2
Reaktionsgleichung
Edukte
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1workup.ALIQUOTA part of the reaction solution was sampled
Vorschrift
A part of the reaction solution was sampled and the components of the reaction solution were analyzed by HPLC, as a result, the concentration of the starting material 2-hydroxyhexanoic acid amide was 1.3 mass % in the solution and the concentration of 5-butyl-oxazolidin-2,4-dione sodium salt as the objective product was 25.9 mass % in the solution. From these analysis values, the conversion of 2-hydroxyhexanoic acid amide was 93.8% and the yield in terms of 5-butyl-oxazolidin-2,4-dione was 88.7%.