Reaktion #10361

Reaktionsgleichung

4,6-dichloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidine

benzylsulfamic acid amide potassium salt

→

Benzylsulfamic acid [6-chloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidin-4-yl]-amide

Ausbeute 47.0%

Reaktionsbedingungen

Vorschrift

Benzylsulfamic acid [6-chloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidin-4-yl]-amide (0.7 g) was prepared from 4,6-dichloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidine (1 g) and benzylsulfamic acid amide potassium salt (1.21 g) according to the procedure described in Referential Example 15. LC-MS: tR=5.13; [M+H]+=456.91.

Quelle