Reaktion #10339

ord-e9f16d4033b3426ca548f02ccc0c2b35

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

According to the procedure described in referential Example 1e), 5-methyl-pyridine-2-sulfamic acid amide (252 mg, Referential Example 20) was reacted with 4,6-dichloro-5-(o-methoxyphenoxy)-2-(4-pyridyl)-pyrimidine (410 mg, Referential Example 1d)) to give 5-methyl-pyridine-2-sulfamic acid-[6-chloro-5-(o-methoxyphenoxy)-2-(4-pyridyl)-4-pyrimidinyl]-amide (100 mg). tR=4.02 min (LC); [M+H]+=499.33 (ES+);

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07094781B2uspto-grants-2006_08