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CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H](NCCCCNCCCN)[C@@]4(O)C[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #92661

5α-Hydroxy-6β-[4-(3-aminopropylamino)-butylamino]-cholestan-3β-ol

Ausbeute 50.4%DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H](NCCCCN)[C@@]4(O)C[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #92662

5α-Hydroxy-6β-(4-aminobutylamino)-cholestan-3β-ol

Ausbeute 61.0%DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H](NCCCN)[C@@]4(O)C[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #92663

5α-Hydroxy-6β-(3-aminopropylamino)-cholestan-3β-ol

Ausbeute 60.0%DOI: 10.6084/m9.figshare.5104873.v1

CCCN[C@@H]1C[C@H]2[C@@H]3CC[C@H]([C@H](C)CCCC(C)C)[C@@]3(C)CC[C@@H]2[C@@]2(C)CC[C@H](O)C[C@]12O

Reaction #92664

5α-Hydroxy-6β-(3-propylamino)-cholestan-3β-ol

Ausbeute 71.5%DOI: 10.6084/m9.figshare.5104873.v1

Reaction #92666

Ausbeute 49.0%DOI: 10.6084/m9.figshare.5104873.v1

CC(=O)O[C@H]1CC[C@]2(C)[C@H]3CC[C@]4(C)[C@@H]([C@H](C)CCCC(C)C)CC[C@H]4[C@@H]3C[C@@H](NCCc3c[nH]cn3)[C@@]2(O)C1

Reaction #92670

5α-Hydroxy-6β-[2-(1H-imidazol-4-yl)-ethylamino]-cholestan-3β-yl acetate

Ausbeute 61.1%DOI: 10.6084/m9.figshare.5104873.v1

CCCC(=O)O[C@H]1CC[C@]2(C)[C@H]3CC[C@]4(C)[C@@H]([C@H](C)CCCC(C)C)CC[C@H]4[C@@H]3C[C@@H](NCCc3c[nH]cn3)[C@@]2(O)C1

Reaction #92671

5α-Hydroxy-6β-[2-(1H-imidazol-4-yl)-ethylamino]-cholestan-3β-yl butyrate

Ausbeute 60.4%DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H](NCCO)[C@@]4(O)C[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #92672

5α-Hydroxy-6β-[2-hydroxyethylamino]-cholestan-3β-ol

Ausbeute 98.0%DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3CC(O)C4=CC(=O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #813710

6-Hydroxy-4-cholesten-3-one

Ausbeute 51.7%DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H]4O[C@@]45C[C@@H](O)CC[C@]5(C)[C@H]3CC[C@]12C

Reaction #1067970

Cholesterol 5α,6α-epoxide

DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H]4O[C@@]45C[C@@H](O)CC[C@]5(C)[C@H]3CC[C@]12C.O=C(O)c1nc[nH]c1C(=O)O

Reaction #1067971

desired product

DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@H]4O[C@]45C[C@@H](O)CC[C@]5(C)[C@H]3CC[C@]12C.O=C(O)c1nc[nH]c1C(=O)O

Reaction #1067972

desired product

DOI: 10.6084/m9.figshare.5104873.v1

C1CCNCC1.CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@@H]4O[C@@]45C[C@@H](O)CC[C@]5(C)[C@H]3CC[C@]12C

Reaction #1067973

desired product

DOI: 10.6084/m9.figshare.5104873.v1

CCCO[C@@H]1C[C@H]2[C@@H]3CC[C@H]([C@H](C)CCCC(C)C)[C@@]3(C)CC[C@@H]2[C@@]2(C)CC[C@H](O)C[C@]12O

Reaction #1067974

6β-n-propoxy-3β,5α-dihydroxycholestane

DOI: 10.6084/m9.figshare.5104873.v1

CC(C)CCC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3CC(O)C4=CC(=O)CC[C@]4(C)[C@H]3CC[C@]12C

Reaction #1544100

6-Hydroxy-4-cholesten-3-one

Ausbeute 51.7%DOI: 10.6084/m9.figshare.5104873.v1

CC(=O)O[C@H]1CC[C@]2(C)[C@H]3CC[C@]4(C)[C@@H]([C@H](C)CCCC(C)C)CC[C@H]4[C@@H]3C[C@H]3O[C@]32C1

Reaction #1847496

5β,6β-Epoxy-3β-acetoxycholestane

DOI: 10.6084/m9.figshare.5104873.v1